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Column: Sample Prep Perspectives
Sample Preparation Perspectives' editor Ron Majors examines technologies and methodologies for getting your samples ready for chromatographic analysis.

The Use of Hollow Fibers in Liquid-Phase Microextraction

August 1, 2010

In this installment, the subject of LPME is reviewed, with emphasis on the use of hollow fibers.

QuEChERS: An Interview with the Inventors

July 1, 2010

The inventors of the QuEChERS technique present an update and a look at the future.

Electromembrane Extraction

March 1, 2010

How the combination of an electroextraction with hollow-fibre liquid-phase microextraction can lead to a selective, rapid method

Electromembrane Extraction

February 1, 2010

How the combination of an electroextraction with hollow-fiber liquid-phase microextraction can lead to a selective, rapid new method.

Salting-out Liquid-Liquid Extraction (SALLE)

July 1, 2009

Ron Majors discusses the technique of Salting-out Liquid-Liquid Extraction (SALLE) and provides some examples of its successful applications.

Stir Bar Sorptive Extraction (SBSE) and Headspace Sorptive Extraction (HSSE): An Overview

May 1, 2009

The guest columnists review SBSE and HSSE and examine their advantages and limitations, along with providing approaches to overcoming the latter.

Practical Aspects of Solvent Extraction

March 1, 2009

Columnist Ron Majors discusses some of the practical considerations in the successful application of the popular yet age-old technique of solvent extraction (also known as liquid–liquid extraction, or LLE). After a brief review of the basics, guidelines on the selection of the appropriate extraction solvents and how to use acid–base equilibria to ensure efficient extractions of ionic and ionizable compounds are provided. Problems in LLE and the solutions to these problems are highlighted. A newer technique called dispersive liquid–liquid microextraction (DLLME) is introduced.

Extraction and Preconcentration of Residues and Contaminants in Food Samples Using Membrane Techniques

February 1, 2009

Guest authors from South Africa review the application of membranes in the extraction, preconcentration, and separation of various contaminants in food.

Practical Aspects of Solvent Extraction

December 1, 2008

Columnist Ron Majors discusses some of the practical considerations in the successful application of the popular yet age-old technique of solvent extraction (also known as liquid–liquid extraction, or LLE).

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