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Content related to sample preparation.

Automating Sample Preparation for MS Analysis of Recombinant Proteins

Jun 1, 2009

A research group from AlbaNova University Center, Royal Institute of Technology (Stockholm, Sweden) developed an automated method for purifying and desalting proteins before mass spectrometry analysis.

SPE of Lipophilic Marine Biotoxins

Jun 1, 2009

A research group from NRL Marine Biotoxins, Federal Institute for Risk Assessment (Berlin, Germany) developed a solid-phase extraction (SPE) method for the enrichment and clean-up of lipophilic marine biotoxins from various species of bivalve molluscs and processed shellfish products.

Liquid-Liquid-Liquid Microextraction of Nerve Agents

Jun 1, 2009

Researchers from Vertox Laboratory, Defence Research and Development Establishment (Gwalior, India) used a liquid-liquid-liquid microextraction technique followed by liquid chromatography?mass spectrometry (LC?MS) to examine alkyl alkylphosphonic acids, which are important environmental markers of nerve agents.

The Continuing Acetonitrile Shortage: How to Combat it or Live with It

Jun 1, 2009

Ron Majors provides an unbiased look at this present crisis and gives alternative solutions.

Collagenase-Assisted Extraction of Pharmaceutical Compounds

Jun 1, 2009

Researchers from Banyu Pharmaceutical Co. (Ibaraki, Japan) used a novel extraction method to prepare drugs in gelatin capsules for analysis by high performance liquid chromatography.

Dispersive Liquid-Phase Microextraction of Aromatic Amines in Water

Jun 1, 2009

Scientists from Henan Normal University (Xinxiang, China) and the University of Science and Technology Beijing (Beijing, China) developed an ultrasound-assisted ionic liquid dispersive liquid-phase microextraction procedure for determining four aromatic amines in water samples.

Stir Bar Sorptive Extraction (SBSE) and Headspace Sorptive Extraction (HSSE): An Overview

May 1, 2009

The guest columnists review SBSE and HSSE and examine their advantages and limitations, along with providing approaches to overcoming the latter.

CE Protein Analysis with Sample Salt Additives

May 1, 2009

Researchers from Uppsala University (Uppsala, Sweden) added alkali salts to protein samples in preparation for capillary electrophoresis (CE) analysis of intact proteins.

Effects of Sample-Dissolving Solvents and Sample Ionic Strength in Routine CE Operation

May 1, 2009

The ionic strength of a sample and the solvent used to dissolve it play a pivotal role in routine capillary electrophoresis (CE).

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